DSC 250

At the core of every Discovery DSC is the NEW TA Fusion Cell™, which incorporates design concepts that “FUSE” together the best features of the world’s bestselling Q-Series and first generation Discovery DSC, patented Tzero® technology, and new proprietary manufacturing processes. Unlike competitive designs, the Discovery DSC delivers optimum performance with a single sensor, eliminating the need to exchange sensors to optimize a specific performance aspect. The result is an innovative new DSC with unrivaled performance in baseline flatness, sensitivity, resolution, and reproducibility.

Features and Benefits:

• Patented Tzero technology measures cell resistance and capacitance characteristics and delivers fundamentally more accurate heat flow measurement, incomparable baseline performance and eliminates baseline corrections prevalent in all other competitive offerings.
• Fixed pedestal-mounted sensor provides a stable configuration with a well-defined and reproducible heat flow path.
• Rugged uniblock Silver furnace with long-life windings ensures superior temperature control and uniformity.
• Unique cooling rods and ring design produce superior cooling performance over a wide temperature range, higher cooling rates, and more responsive heating to cooling operation.
• Temperature-controlled electronics ensure the utmost in stability and repeatability of measured signals.
• Innovative Gas-Delivery manifold provides gas switching and consistent, repeatable atmosphere.

The new Fusion cell delivers the purest real-time heat flow data possible. Additionally, lengthy pre and post-test manipulations, such as baseline subtractions or de-smearing routines by required competitive designs are never necessary.

Traditionally, DSC heat flow measurements have been based on the same principle that ASSUMES contributions by the sample and reference sensor to the total measured heat flow simply cancel each other out. If this assumption was true, all DSC’s would have perfectly flat baselines. In reality, they do not. The fact is that each sensor’s resistance and capacitance (ability to store energy) produce imbalances in the heat flow, resulting in deviations from baseline flatness and impaired resolution and sensitivity. ONLY TA Instruments, with patented Tzero Technology, can measure this imbalance. Tzero Technology eliminates complicated pre- and post-test manipulations, such as baseline subtraction, deconvolution or other mathematical treatments competitive designs must use to improve baseline performance, sensitivity and resolution.

Patented Tzero Technology measures the resistance and capacitance of the sensors and utilizes these values in the four-term heat flow equation to give the most accurate real-time determination of heat flow available on any DSC. TA engineers have taken this one step further by also including the contributions of the DSC pans. This Advanced Tzero technology, T4P heat flow, provides the sharpest resolution, the highest sensitivity and allows for the measurement of heat capacity in a single run!

Tzero Features and Benefits:

• Flattest baselines available of any DSC on the market, resulting in the
  purest data without manipulation or subtraction.
• Highest resolution and sensitivity, without ever needing lengthy pre- and
  post-test manipulations as required by competitive designs.
• Direct measurement of heat capacity delivering the most uniform and
  accurate heat flow to and from the sample.
• By improving every aspect of performance, the Discovery DSC delivers data
  the user can trust, in all applications, all the time.

DISCOVER more Accurate Data with patented Tzero™ Technology

In patented TA MDSC®*, a sinusoidal temperature oscillation is overlaid on the traditional linear ramp. The net effect is that heat flow can be measured simultaneously with, and independently of, changes in heat capacity. The Total Heat Flow signal contains the sum of all thermal transitions, just as in standard DSC. The Reversing Heat Flow contains glass transition and melting transitions, while the Nonreversing Heat Flow contains kinetic events like curing, volatilization, melting, and decomposition. TA invented MDSC and understands it like no other company. Modulated DSC is standard on EVERY Discovery DSC model.

Benefits of MDSC include:

• Separation of complex and overlapping transitions into more easily interpreted components.
• Increased sensitivity for detecting weak transitions.
• Increased resolution without loss of sensitivity.
• More accurate measurement of polymer crystallinity.
• Direct measurement of heat capacity.

* U.S. Patent No. 6,561,692

It’s hard to believe we could improve on the most reliable DSC autosampler on the market, but we did! The new linear autosampler was designed to be even more rugged and simple to use than ever before, while offering maximum in testing flexibility.

Autosampler Features and Benefits:

• New Linear X-Y-Z design with integrated auto lid reduces sample loading time for increased throughput and reliability.
• The integrated auto lid gives consistent and repeatable cell closure further improving the repeatability of measurements.
• New laser positioning system enables one-touch automatic calibration and pan location verification.
• Scheduled and unattended calibrations and verifications gives scientists more time for research.
• New TRIOS software makes it easier than ever to manage and run a large and diverse sample queue.
• The Design view and Running queue allow for quick and efficient autosampler programming.
• Sample and reference pans may be assigned to any combination of the available 54 positions.
• Includes two quick-change trays for more convenient remote sample preparation.
• Convenient design allows the choice of unloading pans back to the tray, or disposing of them freeing space for continuous sample queuing.

All Discovery DSC’s feature the innovative “app-style” touch screen. This makes operation easier than ever, with enhanced One-Touch-Away™ functionality. As easy as operating a tablet or smart phone!

Touch Screen Features and Benefits:

• Ergonomic design for easy viewing and operation
• Packed with functionality to simplify operation and enhance user experience.
  The apps-style touch screen includes:

• Start stop runs
• Test and instrument status
• Real-time signals
• Real-time plot
• Active method viewing
• Advance method segments
• Autosampler calibration
• Loading/unloading pans
• System information

The app-style touch screen, powerful new TRIOS software, the robust and reliable
autosampler with automated calibration and verification routines all work seamlessly to dramatically improve laboratory workflow and productivity.

Refrigerated Cooling Systems (RCS)
Full line of cooling systems, designed and manufactured by TA Instruments,
specifically for our DSC’s, featuring the new RCS 120 three-stage refrigerated system capable of temperatures down to -120°C.

RCS Features and Benefits:
• One-, Two-, or Three-stage refrigeration system that achieves
temperature ranges down to -120°C.
• Sealed system eliminates the need for LN2 cooling system.
• Enables cycling, MDSC®, controlled and ballistic cooling
experiments.
• Safe, convenient, and continuous cooling operation for your
laboratory needs.

The FACS is an innovative cooling accessory that offers a cost-effective alternative to the RCS or LN2P cooling systems. The FACS can be used for controlled cooling experiments, thermal cycling studies, and to improve sample turnaround time. Stable baselines and linear heating and cooling rates can be achieved between ambient and 725°C.

Autosampler

The DSC 25 and DSC 250 non-Auto systems can be field retrofitted to the 54-position autosampler.

Autosampler Features and Benefits:

• New Linear X-Y-Z design with integrated auto lid reduces sample loading time for increased throughput and reliability.
• The integrated auto lid gives consistent and repeatable cell closure further improving the repeatability of measurements.
• New laser positioning system enables one-touch automatic calibration and pan location verification.
• Scheduled and unattended calibrations and verifications gives scientists more time for research.
• New TRIOS software makes it easier than ever to manage and run a large and diverse sample queue.
• The Design view and Running queue allow for quick and efficient autosampler programming.
• Sample and reference pans may be assigned to any combination of the available 54 positions.
• Includes two quick-change trays for more convenient remote sample preparation.
• Convenient design allows the choice of unloading pans back to the tray, or disposing of them freeing space for continuous sample queuing.

The LN2P provides the highest performance and greatest flexibility in cooling for the Discovery DSC. It facilitates the lowest operational temperature (to -180 °C), greatest cooling rate capacity (to 140 °C/min), fastest sub-ambient equilibration times, and an upper temperature limit of 550 °C. Operating at ambient pressure, the LN2P uses liquid nitrogen efficiently, thus reducing operating costs. It includes a 50-liter Dewar with auto-fill capability which allows the LN2P to be automatically refilled from a larger source, even during a DSC experiment, for continuous DSC operation with no disruption.

Proper sample preparation is of critical importance to the quality of data generated on a DSC. The Tzero sample encapsulation press and pans take into consideration every detail necessary by design to ensure simple and proper preparation for the highest data quality.

Tzero high-performance pans and lids are designed to maximize pan flatness and sample contact. Coupled with the unparalleled flatness and uniformity of the Fusion cell sensor, the Tzero pans and lids provide the most direct, uniform heat flow path from the sample to the sensor. These pans are tolerant of many sample forms and are designed with lids that conform to the top of irregular specimens, efficiently transferring heat to and from the entire sample. Competitive pan designs that have non-flat bases are unable to achieve appropriate thermal contact with solid specimens. Fabricated using advanced technology and to extremely tight tooling specifications, the Tzero pans offer significant improvements in resolution and repeatability over any other pan design.

Tzero® DSC Sample Encapsulation Press
The Tzero press takes sample encapsulation to a higher level of performance and convenience in conventional and hermetic sealing of a wide variety of materials. The press kit includes four die sets for Tzero aluminum and hermetic pans & lids. Optional die sets are available for high-volume DSC pans and Discovery TGA sealed pans. The die sets are magnetically attached with no tools or adjustments required. In addition, each die set is color-coded to the box containing the compatible Tzero or standard aluminum hermetic pans and lids.

The Photocalorimeter Accessory (PCA) permits characterization of photocuring materials between -50 and 250°C. UV/Visible light (320-500 nm) from a 200 W high pressure mercury source is transmitted to the sample chamber via an extended range, dual-quartz light guide with neutral density or band pass filters. Tzero® technology permits direct and accurate measurement of light intensity at both the sample and reference positions without the need for an external radiometer. It also provides for simultaneous measurement of two samples.

The Optical Accessory Kit provides the capabilities for measuring the calorimetric characteristics of a sample, such as heat flow and heat capacity, while simultaneously collecting information on the optical characteristics, such as Raman, Near-IR and visible changes in the sample. Such measurements can provide information on the chemical or structural changes that are occurring within a material that is complementary to the heat flow data collected by the DSC. A specially designed cell lid assembly allows for direct observation of the sample by the external optical probe while maintaining high-quality calorimetric performance. This flexible interface can be configured to work with many optical systems through the use of an appropriate probe adapter supplied by any 3rd-party vendor.

Discovery DSC Microscope Accessory

DSC thermograms can sometimes be complicated and difficult to interpret. On many occasions, multiple DSC experiments must be performed to better understand a thermal event. The Discovery DSC Microscope Accessory allows the user to easily view the sample while performing a DSC experiment. This accessory aides in the identification of endothermic solid-solid phase transitions that may erroneously be interpreted as melting endotherms. Furthermore, the experimenter can now observe physical changes in a material as it undergoes phase transitions and volumetric dimensional changes, such as shrinkage, associated with a transition, evaporation or sublimation.

The Discovery DSC Microscope Accessory is a high resolution digital microscope camera which simultaneously captures images and video during a DSC experiment.

Discovery DSC Microscope Features and Benefits

• The Discovery DSC Microscope Accessory can be used with any of the new Discovery DSC 2500, 250 and 25 instruments
• It is compatible with the LN pump, FACS and RCS cooling accessories for a wide operational temperature range of -180 to 725 °C
• The accessory is user-installable and is quickly installed when needed to study a material
• 3 method segments (Image Capture, Video and Dynamic Video) make it easier than ever to simultaneously capture images and video in a single experiment. Dynamic Video is a unique command used to capture video clips only when a heat flow thermal event in the test sample is detected. This helps reduce the size of the video footage by not capturing video during inactive heat flow time periods

DSC performed with the microscope accessory has several applications that may prove insightful to better understanding materials’ properties and behaviors. It allows the scientist to capture images of:

• crystallization and melt transitions
• flow of materials above the glass transition and melting point
• volumetric, dimensional changes associated with a phase transition, evaporation and sublimation
• visual observations of coloration and other deviations in appearance

Unleash the full potential of your research with TA Instruments – Waters Corporation’s state-of-the-art LED Photocalorimeter Accessory (LED-PCA). Engineered for precision and innovation, the LED-PCA allows for the comprehensive study and characterization of photocurable materials across a broad temperature spectrum from -50°C to 250°C. Embrace the future of research technology with the LED Photocalorimeter Accessory (LED-PCA) from TA Instruments.

Key Features:

• Temperature Optimization: Explore a dynamic operational temperature range from -50°C to 250°C, empowering you to fine-tune reaction conditions, including intensity, wavelength, temperature, atmosphere, and exposure time.
• Mercury-Free Environment: In alignment with the Minamata Convention, our LED-PCA eliminates the need for mercury lamps, providing a safer and cleaner laboratory environment.
• Wavelength Precision: Choose from precise LED wavelengths at 365nm, 385nm, 395nm, and 405nm. Tailor your experiments with intensity control ranging from 5 mW/cm2 to >10 W/cm2, typically falling within 10-100 mW/cm2.
• Intuitive Control: Manage intensity effortlessly through the OmniCure® LX500 source, two neutral density filters, and fine-tuning screws on the accessory itself, ensuring unmatched control over your experiments.
• TA Instruments Tzero^TM Technology: Experience direct, accurate, and real-time measurement and matching of UV light intensity at both sample and reference positions. Our touchscreen interface helps eliminate the need for an external radiometer and helps ensure consistent light intensity throughout numerous sample measurements.

Additional Features:

• Versatile Applications: Ideal for materials science, polymers, paints and CASE, electronics, food, pharmaceuticals and healthcare, cosmetics, and more.
• Extended Instrument Lifetimes: LED UV sources guarantee substantially longer lifetimes and maintain intensity, surpassing the performance of traditional mercury lamps.
• Transform your research landscape with the LED-PCA. Elevate your experiments today!

TRIOS EasyMass Software: Streamlining Sample Preparation and Enhancing Accuracy

TRIOS™ EasyMass Software revolutionizes your laboratory workflow by seamlessly integrating your balance with TRIOS software to capture sample weights directly. Learn more about how TRIOS EasyMass Software can enhance your differential scanning calorimetry (DSC) tests:

1. Direct Electronic Mass Data Transfer Minimizes Errors
   Bid farewell to manual transcription and calculation mishaps. TRIOS EasyMass Software enables direct digital transfer of mass data from the balance into TRIOS Software, ensuring accuracy and reliability.
2. Eliminate Pencil and Paper
   Traditional sample preparation often involves scribbling measurements on paper. With our solution, you can go paperless, streamlining your workflow and reducing clutter.
3. Boost Productivity with Seamless Integration
   Repetitive tasks become a breeze. TRIOS EasyMass Software seamlessly transfers data, allowing you to focus on higher-value work. No more wasted time on manual data entry.
4. Intuitive User Guidance
   Both TRIOS Software and the balance display provide intuitive guidance, ensuring that essential data is captured accurately. New users will appreciate the reduced training time.
5. Streamlined Experiment Repetition
   For each DSC run in the queue, your sample data is automatically entered. Need to repeat the same method on multiple samples? It’s as simple as a click, saving you valuable time.
6. Enhanced Review and Auditing
   Facilitate reliable second-person reviews and auditing. TRIOS EasyMass Software helps to ensure that data is associated with the relevant TRIOS Software user, enhancing accountability and traceability.

Elevate your DSC experiments to new heights of efficiency with TRIOS EasyMass Software. Say goodbye to manual drudgery and hello to seamless data flow!

JSON Export: The Future of Data Management

• Seamless Integration: Convert your TRIOS data into the open standard JSON format, making it easy to integrate with programming tools, data science workflows, and lab systems (e.g. LIMS). JSON is available:
  • Automatically on every save (enabled in options)
  • Through manual export dialogs
  • As part of the “Send to LIMS” functionality
  • Via the “Batch” processing dialog or from the command line
  • In TRIOS AutoPilot
• Data Consistency: Our publicly available JSON schema ensures a consistent data structure, allowing you to write code once and apply it universally across all your data files.
• Python Library: Use our open-sourced python library, TA Data Kit, to simplify your data ingestion or learn how to take advantage of the power of our data with our code examples.

For more information, click here

Polymer Guided Methods

Guided Methods for Initial Crystallinity, Glass Transitions, Percent Cure, and Thermal Transitions provide an easy-to-use interface for new users to obtain desired results with minimal training. 

Initial Crystallinity  

• Preconfigured ramp templates with customizable ramp rates and start/end temperatures 
• Automatically calculates and reports the crystallinity using the 100% crystalline value 

Glass Transitions  

• Preconfigured ramp templates with customizable ramp rates and start/end temperatures 
• Automatically intelligently analyzes and reports all thermal transitions and prompts the user with the glass transition value(s) 

Percent Cure  

• Preconfigured ramp templates with customizable ramp rates and start/end temperatures 
• Automatically calculates and reports the percent cure using the 100% cure enthalpy value 

Thermal Transitions  

• Consists of two separate methods, one for a single heat and another for a heat-cool-heat cycle 
• Preconfigured ramp templates with customizable ramp rates and start/end temperatures 
• Automatically intelligently analyzes and reports all thermal transitions in both heat steps