Measurement of Glass Transition Temperatures by Dynamic Mechanical Analysis and Rheology
This note will detail the use of dynamic mechanical analysis (DMA) and rheology to characterize the glass transition of a polymeric material.
DetailsView allAdhesives & SealantsApplication NotesApplicationsArchiveARES G2 AccessoriesARES RheometerAutomated Density TesterAutomated Hardness TesterBatteriesBatteries & Battery MaterialsBatteriesBatteriesBiopharmaBiopharmaceuticalsBlog ApplicationsBlog Techniquescardiovascular instrumentsCase StudiesCeramicsCompositesCompositesDHR AccessoriesDifferential Scanning CalorimetersDifferential Scanning CalorimetryDIL 830 SeriesDilatometersDilatometry videosDilatometryDilatometryDiscovery Hybrid RheometersDraftsDynamic Mechanical Analysis (DMA)Dynamic Mechanical AnalyzersDynamic Mechanical Analyzers (DMA)Dynamic Mechanical Analyzers (Rheology)Dynamic Mechanical Analyzers (Thermal Analysis)ElastomersElectroForceElectroForceElectroForce NotesElectroForceElectroForceElectroForceElectronic Materials & ProductsElectronicsEnd of Life ProductsEngineered MaterialsFine & Specialty ChemicalsFlash Diffusivity SystemsFlash DiffusivityFlash Diffusivity VideosFood ProductsGeneralGlass ProductsGuarded heat flow meterHeating MicroscopesHigh Pressure AnalyzersHigh Throughput DSCHorizontal DilatometersIn-Person TrainingInorganics - OtherInorganics - MineralsInsulation & Building MaterialsIsothermal CalorimetryIsothermal Titration CalorimetryLaser FlashLoad frame systemsMaterial CharacterizationMechanical TestingMechanical TestingMedical Device TestingMedical DevicesMetals ProductsMicrocalorimetry videosMicrocalorimetryMicrocalorimetryMicrocalorimetryMicrocalorimetry NotesMicrocalorimetryMooney ViscometerMoving Die RheometerMulti-Specimen FatigueNews & InfoOils, Lubricants, & FluidsOptical DilatometersOptical FleximeterOrganic Chemicals & ProductsPaints, Inks, & CoatingsPercarbonatesPersonal Care & Household ProductsPetroleum ProductsPharmaceuticalsPharmaceuticalsPolymersPolymersprivateProduct videosProductsPromotionsQ SeriesQuenching DilatometersQuick start guidesRheology videosRheologyRheologyRheology AccessoryRheologyRheology NotesRheologyRotational ViscometerRubberRubber AccessoriesRubberRubber Process AnalyzersRubberRubber TestingRubber TestingRubber TestingRubothermSeminarsService VideosSimultaneous Thermal AnalyzerSoftwareSoftwareTA Quick Talk VideosTech TipsTestbench and Planar Biaxial systemsThermal Analysis videosThermal AnalysisThermal AnalysisThermal Analysis NotesThermal AnalysisThermal ApplicationsThermal Conductivity & DiffusivityThermal Conductivity MeterThermal ConductivityThermal Conductivity VideosThermogravimetric AnalysisThermomechanical AnalyzersThermophysical NotesThermophysical Properties NotesTrainingUncategorizedVapor Sorption AnalysisVertical DilatometersVideosDilatometryWebinarsMicrocalorimetryRheologyRubberThermal AnalysisXenon Flash
Thermal Degradation Study of Nylon 66 using Hyphenation Techniques TGA-MS and TGA-FTIR-GC/MS
In this work, the thermal degradation process of nylon 66 was studied using TGA-MS, TGA-FTIR and TGA-GC/MS in inert gas environments. These techniques together can provide a lot of insights of the thermal degradation process and its off-gas products.
Details
Powder Flow Measurement on the Discovery Hybrid Rheometer
Overview In this Tech Tip, we will set up the TA Instruments powder rheology flow cell.
DetailsEffect of Thermal Degradation on Polymer Thermal Properties
In this Applications note, we demonstrate using TGA to precisely control the degree of degradation to be < 5wt% and characterize the impact of degrees of degradation on polymer thermal properties.
DetailsEstimation of Polymer Lifetime by TGA Decomposition Kinetics
Thermogravimetric Analysis (TGA) provides a method for accelerating the lifetime testing of polymers so that short term experiments can be used to predict in-use lifetime.
DetailsMedical Devices Regulatory Pathway Download
E-Book Medical Devices Regulatory Pathway Download The Importance of Chemical and Material Characterization Whether increasing efficacy and reliability, reducing manufacturing costs, or delivering the highly personalized devices of the future, the medical devices industry depends on materials science to deliver products that are fit for their intended use and that also meet both regulatory and…
DetailsComparison of the Thermal Behavior of Different Types of Recycled PET for Advanced Honeycomb Structures
This note describes the importance of DSC to study crystallization behavior and crystallinity of recycled PET used in the production of honeycomb structures.
DetailsSemi-Crystalline Thermoplastic Analysis Using the Discovery X3 DSC
This Applications Note discusses the advantages of the Discovery X3 DSC for thermoplastic analysis which includes the ability to identify potential differences in thermal properties as a function of thermal history.
DetailsModulated DSC of a Polypropylene Battery Separator
Modulated DSC (MDSC) was performed on a polypropylene (PP) battery separator to gain additional insights into the effects of stretching during processing of the film.
DetailsModulated Thermomechanical Analysis (MTMA) of Polypropylene Battery Separator Film
Modulated thermomechanical analysis (MTMA) was performed on a polypropylene (PP) battery separator to gain further insight into the mechanism of the dimension change and coefficient of linear expansion (CLE or α).
DetailsPowder Rheology of Graphite: Characterization of Natural and Synthetic Graphite for Battery Anode Slurries
The TA Instruments Powder Rheology Accessory was used with Discovery HR 30 rheometer to perform shear measurements. Duplicate measurements were performed with fresh samples under ambient conditions.
DetailsRheological and Thermogravimetric Characterization on Battery Electrode Slurry to Optimize Manufacturing Process
In this application note, a TA Discovery HR rotational rheometer facilitates coating optimization by measuring slurry viscosity over different shear rates that relate to coating speed. Drying kinetics are investigated with a Discovery TGA to yield the most cost-efficient condition.
Details