Ensuring Patient Safety with Medical Device Testing

Medical devices play a significant role in the quality of health and well-being of patients globally. From adhesive bandages to heart valves, medical devices are used in the diagnosis, prevention, monitoring, and treatment of a broad range of medical conditions. Since these devices have many interactions with patients’ bodies and activities, medical device manufacturers must confirm that their respective products are built to operate with exceptional performance and reliability.

Improving the quality of life for those with chronic diseases like cancer and diabetes, as well as our aging population, has increased demand for high-performance medical devices while adhering to key regulations. As you work to develop novel medical devices, use TA Instruments to optimize and validate product performance and safety.

Analytical Testing for Medical Device Development Pathway

Before complete medical devices are implanted into patients, the development path from product idea to the final device is far from quick and easy.

The medical device development pathway – benchmarking native tissues, characterizing biomaterials and device materials, measuring the reliability of device subcomponents, and testing the efficacy and durability of complete devices – requires testing rigor enabled by precise and reliable instruments. Developing high-performing medical devices depends on the quality of your lab and measurements.

Explore each category in the medical device development pathway for more information.

 

Characterizing Native Tissue

Investigating the behaviors of native tissues offers insights into natural or diseased tissue performance, allowing device developers to explore how these qualities translate into medical device functions. Similarly, techniques for tissue characterization can be leveraged for engineered tissue.

Many tissue-engineered medical products (TEMPs) can be assessed for properties such as mechanical stiffness, compliance, strength, or stability using the same instruments used for native tissue.

Investigate tissue behaviors to develop high-performing medical devices with TA Instruments solutions.

ElectroForce 5500

  • Cartilage, Tendons (of animal models), Ligaments (of animal models)
    • Strength
    • Stiffness
    • Durability
    • In Vivo Loading

ElectroForce 3200

  • Cartilage, Bone, Dentin/Teeth
    • Strength
    • Stiffness
    • Durability
  • Spinal Cord and Nerves
    • Strength
    • Stiffness
    • Response to injury

ElectroForce 3300

  • Muscle
    • Strength
    • Stiffness
    • Response to Stimulus
  • Bone, Dentin/Teeth
    • Strength
    • Stiffness
    • Durability

ElectroForce 3500

  • Bone, Tendon, Ligament
    • Strength
    • Stiffness
    • Durability

TestBench and Planar Biaxial

  • Heart valve leaflets, Pericardium
    • Strength
    • Stiffness
    • Durability
    • Anisotropy
  • Skin
    • Strength
    • Stiffness
    • Anisotropy

Characterizing Biomaterials and Device Materials

A biomaterial is any synthetic material used in the replacement or restoration of body tissue functions. Since biomaterials and other device materials are used in developing medical devices, it is essential to understand how biomaterials and other components contribute to final medical device functions. Most materials used for medical device construction are classified under metals, ceramics, polymers, and composites.

Investigate material properties relevant to medical device construction with TA Instruments solutions.

Thermogravimetric Analysis

  • Polymers
    • Volatiles
    • Thermal and Oxidative Stability
    • Kinetics
    • Lifetime Prediction
    • Composition Information
    • Residue

ElectroForce 3200

  • Hydrogels
    • Stiffness
    • Modulus
    • Creep-Recovery
  • Contact Lens
    • Lubrication
  • Shape Memory Alloys (SMA)
    • Thermal Cycling for Transitions
DMA beauty

Dynamic Mechanical Analysis

  • Polymers
    • Glass Transition
    • Effect of Plasticization
    • Effect of Humidity
    • Mechanical Properties
    • Thermal Cycling
  • Hydrogels
    • Creep-Recovery

Thermomechanical Analysis

  • Polymers
    • Glass Transition
    • Coefficient of Thermal Expansion (CTE)
    • Curing
    • Effect of Plasticization

Multi-Specimen Fatigue

  • Nickel-Titanium Super-elastic Materials
    • Fatigue-to-Fracture
    • S-N Curves
    • Fatigue Life Curves
  • Other High Purity Metal Stent Wire
    • Fatigue-to-Fracture of Z-Shape Samples

ElectroForce 3300

  • Bone Cement
    • Fatigue and Durability
DSC beauty

Differential Scanning Calorimetry

  • Polymers
    • Glass Transition
    • Amorphous content
    • Curing
    • Cure reactions
    • Effect of Plasticization
    • Enthalpic Recovery/Aging
    • Melting
      • Degree of crystallinity
      • Crystalline morphology
    • Crystallization
    • Solid Phase Changes
  • Shape Memory Alloys (SMAs)
    • Transition temperatures
DHR beauty

Rheometry

  • Adhesives
    • Temperature ramp tests
    • Axial or Tack Testing
    • Shrinkage
    • UV curing
  • Hydrogels
    • Gel time
    • Gel strength
    • Isothermal and non-isothermal gelation
    • Creep-Recovery

Fatigue Tests of Device Subcomponents

Each subcomponent used for medical device manufacturing comes with various properties that contribute to the success of the complete device. Understanding how the characteristics of each subcomponent can affect the performance and overall reliability of the complete device is very important to the final stage of the medical device development pathway. Furthermore, subcomponent failure analysis and testing are becoming an increasingly beneficial and requested element of regulatory submissions. Examples of device subcomponents are diamonds and frames, bone screws, dental screws, pacemaker leads, and many more.

Investigate fatigue properties of your medical device subcomponents with TA Instruments solutions

Multi-Specimen Fatigue

  • Stent subsections (diamond surrogates)
    • Fatigue-to-Fracture
    • Fatigue Test-to-Success
  • Pacemaker and Defibrillator Leads
    • Fatigue-to-Fracture
    • Fatigue Test-to-Success
  • IVC Filters
    • Fatigue-to-Fracture

ElectroForce 3200

  • Pacemaker Cans and Connectors
    • Fatigue and Durability
    • Connector Reliability

ElectroForce 3300

  • Bone Screws
    • Strength
    • Insertion Torque
    • Pull-out Strength
  • Dental Screws
    • Strength
    • Insertion Torque
    • Pull-out Strength
  • Orthopedic Device Connections
    • Strength
    • Durability
  • Dental Crowns
    • Wear properties

DuraPulse SGT

  • Stents of Transcatheter Heart Valves (TAVR)
    • Pulsatile durability
    • Fatigue-to-Fracture

Fatigue Tests of Complete Devices

Testing complete devices verifies reliability and performance based on the end-use application. Ensuring that the final product meets specifications with utmost performance without compromising patient safety is critical to the success of the overall product development and regulatory submissions. ASTM and ISO standards include exact measurements of complete device behaviors, which can be measured on-the-bench with TA Instruments. Examples of complete devices are heart valves, stent/grafts, contact lenses, dental implants, spinal implants, and many more.

Investigate fatigue properties of your complete medical device with TA Instruments solutions

ElectroForce 3200

  • Contact lenses
    • Friction
    • Lubricity

DuraPulse HVT

  • Transcatheter Heart Valves (TAVR)
    • Accelerated Wear Test (AWT)
  • Surgical Heart Valves
    • Accelerated Wear Test (AWT)

ElectroForce 3300

  • Dental Implant
    • Axial Fatigue
  • Spinal Implant
    • Axial Fatigue
    • Axial-Torsion Fatigue

ElectroForce 3500

  • Hip Implants
    • Axial Fatigue
    • Axial-Torsion Fatigue
  • Breast Implant
    • Axial Fatigue

Multi-Specimen Fatigue

  • IVC Filters
    • Axial-Radial Durability
  • Other cardiovascular devices
    • Axial Durability

DuraPulse SGT

  • Stent or Stent/Grafts
    • Pulsatile durability
    • Fatigue-to-Fracture
  • IVC Filters
    • Radial durability
Native Tissue

Characterizing Native Tissue

Investigating the behaviors of native tissues offers insights into natural or diseased tissue performance, allowing device developers to explore how these qualities translate into medical device functions. Similarly, techniques for tissue characterization can be leveraged for engineered tissue.

Many tissue-engineered medical products (TEMPs) can be assessed for properties such as mechanical stiffness, compliance, strength, or stability using the same instruments used for native tissue.

Investigate tissue behaviors to develop high-performing medical devices with TA Instruments solutions.

ElectroForce 5500

  • Cartilage, Tendons (of animal models), Ligaments (of animal models)
    • Strength
    • Stiffness
    • Durability
    • In Vivo Loading

ElectroForce 3200

  • Cartilage, Bone, Dentin/Teeth
    • Strength
    • Stiffness
    • Durability
  • Spinal Cord and Nerves
    • Strength
    • Stiffness
    • Response to injury

ElectroForce 3300

  • Muscle
    • Strength
    • Stiffness
    • Response to Stimulus
  • Bone, Dentin/Teeth
    • Strength
    • Stiffness
    • Durability

ElectroForce 3500

  • Bone, Tendon, Ligament
    • Strength
    • Stiffness
    • Durability

TestBench and Planar Biaxial

  • Heart valve leaflets, Pericardium
    • Strength
    • Stiffness
    • Durability
    • Anisotropy
  • Skin
    • Strength
    • Stiffness
    • Anisotropy
Biomaterials

Characterizing Biomaterials and Device Materials

A biomaterial is any synthetic material used in the replacement or restoration of body tissue functions. Since biomaterials and other device materials are used in developing medical devices, it is essential to understand how biomaterials and other components contribute to final medical device functions. Most materials used for medical device construction are classified under metals, ceramics, polymers, and composites.

Investigate material properties relevant to medical device construction with TA Instruments solutions.

Thermogravimetric Analysis

  • Polymers
    • Volatiles
    • Thermal and Oxidative Stability
    • Kinetics
    • Lifetime Prediction
    • Composition Information
    • Residue

ElectroForce 3200

  • Hydrogels
    • Stiffness
    • Modulus
    • Creep-Recovery
  • Contact Lens
    • Lubrication
  • Shape Memory Alloys (SMA)
    • Thermal Cycling for Transitions
DMA beauty

Dynamic Mechanical Analysis

  • Polymers
    • Glass Transition
    • Effect of Plasticization
    • Effect of Humidity
    • Mechanical Properties
    • Thermal Cycling
  • Hydrogels
    • Creep-Recovery

Thermomechanical Analysis

  • Polymers
    • Glass Transition
    • Coefficient of Thermal Expansion (CTE)
    • Curing
    • Effect of Plasticization

Multi-Specimen Fatigue

  • Nickel-Titanium Super-elastic Materials
    • Fatigue-to-Fracture
    • S-N Curves
    • Fatigue Life Curves
  • Other High Purity Metal Stent Wire
    • Fatigue-to-Fracture of Z-Shape Samples

ElectroForce 3300

  • Bone Cement
    • Fatigue and Durability
DSC beauty

Differential Scanning Calorimetry

  • Polymers
    • Glass Transition
    • Amorphous content
    • Curing
    • Cure reactions
    • Effect of Plasticization
    • Enthalpic Recovery/Aging
    • Melting
      • Degree of crystallinity
      • Crystalline morphology
    • Crystallization
    • Solid Phase Changes
  • Shape Memory Alloys (SMAs)
    • Transition temperatures
DHR beauty

Rheometry

  • Adhesives
    • Temperature ramp tests
    • Axial or Tack Testing
    • Shrinkage
    • UV curing
  • Hydrogels
    • Gel time
    • Gel strength
    • Isothermal and non-isothermal gelation
    • Creep-Recovery
Subcomponents

Fatigue Tests of Device Subcomponents

Each subcomponent used for medical device manufacturing comes with various properties that contribute to the success of the complete device. Understanding how the characteristics of each subcomponent can affect the performance and overall reliability of the complete device is very important to the final stage of the medical device development pathway. Furthermore, subcomponent failure analysis and testing are becoming an increasingly beneficial and requested element of regulatory submissions. Examples of device subcomponents are diamonds and frames, bone screws, dental screws, pacemaker leads, and many more.

Investigate fatigue properties of your medical device subcomponents with TA Instruments solutions

Multi-Specimen Fatigue

  • Stent subsections (diamond surrogates)
    • Fatigue-to-Fracture
    • Fatigue Test-to-Success
  • Pacemaker and Defibrillator Leads
    • Fatigue-to-Fracture
    • Fatigue Test-to-Success
  • IVC Filters
    • Fatigue-to-Fracture

ElectroForce 3200

  • Pacemaker Cans and Connectors
    • Fatigue and Durability
    • Connector Reliability

ElectroForce 3300

  • Bone Screws
    • Strength
    • Insertion Torque
    • Pull-out Strength
  • Dental Screws
    • Strength
    • Insertion Torque
    • Pull-out Strength
  • Orthopedic Device Connections
    • Strength
    • Durability
  • Dental Crowns
    • Wear properties

DuraPulse SGT

  • Stents of Transcatheter Heart Valves (TAVR)
    • Pulsatile durability
    • Fatigue-to-Fracture
Complete Devices

Fatigue Tests of Complete Devices

Testing complete devices verifies reliability and performance based on the end-use application. Ensuring that the final product meets specifications with utmost performance without compromising patient safety is critical to the success of the overall product development and regulatory submissions. ASTM and ISO standards include exact measurements of complete device behaviors, which can be measured on-the-bench with TA Instruments. Examples of complete devices are heart valves, stent/grafts, contact lenses, dental implants, spinal implants, and many more.

Investigate fatigue properties of your complete medical device with TA Instruments solutions

ElectroForce 3200

  • Contact lenses
    • Friction
    • Lubricity

DuraPulse HVT

  • Transcatheter Heart Valves (TAVR)
    • Accelerated Wear Test (AWT)
  • Surgical Heart Valves
    • Accelerated Wear Test (AWT)

ElectroForce 3300

  • Dental Implant
    • Axial Fatigue
  • Spinal Implant
    • Axial Fatigue
    • Axial-Torsion Fatigue

ElectroForce 3500

  • Hip Implants
    • Axial Fatigue
    • Axial-Torsion Fatigue
  • Breast Implant
    • Axial Fatigue

Multi-Specimen Fatigue

  • IVC Filters
    • Axial-Radial Durability
  • Other cardiovascular devices
    • Axial Durability

DuraPulse SGT

  • Stent or Stent/Grafts
    • Pulsatile durability
    • Fatigue-to-Fracture
  • IVC Filters
    • Radial durability

Commonly Used Testing Standards

  1. ASTM E794 Test Method for Melting and Crystallization Temperatures by Thermal Analysis
  2. ASTM E1356 Test Method for the Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry
  3. ASTM E1641 Test Method for Decomposition Kinetics by Thermogravimetry Using the Flynn/Wall/Ozawa Method
  4. ASTM E2550 Test Method for Thermal Stability by Thermogravimetry
  5. ASTM D5023 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Flexure (Three-Point Bending)
  6. ASTM E831 Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis
  7. ASTM D5279 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Torsion
  8. ISO 14801 Dentistry — Implants — Dynamic loading test for endosseous dental implants 
  9. ASTM F3211 Standard Guide for Fatigue-to-Fracture (FtF) Methodology for Cardiovascular Medical Devices
  10. ASTM F2477 Pulsatile stent testing: Standard Test Methods for in vitro Pulsatile Durability Testing of Vascular Stents

Don’t see what you’re looking for? Click here to explore a comprehensive list of ASTM/ISO standards for your material testing needs. 

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